National Institute for Occupational Safety and Health

Summary

National Institute for Occupational Safety and Health NIOSH Manual of Analytical Methods… (1994)

Bias can also be caused in a cyclone by the pulsation of the personal sampling pump. Bartley, et al. [12] showed that cyclone samples with pulsating flow can have negative bias as large as −0.22 relative to samples with steady flow. The magnitude of the bias depends on the amplitude of the pulsation at the cyclone aperture and the dust size distribution. For pumps with instantaneous flow rates within 20% of the mean, the pulsation bias magnitude is less than 0.02 for most dust size distributions encountered in the workplace. Electric charges on the dust and the cyclone will also cause bias.
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National Institute for Occupational Safety and Health NIOSH Manual of Analytical Methods… (1994)

APPENDIX: Jarless Method for Calibration of Cyclone Assemblies This procedure may be used in the field to calibrate an air sampling pump and a cyclone assembly without using the one-liter “calibration jar”. 1.
Connect the pump to a pressure gauge or water manometer and a light load (adjustable valve or 5-μm filter) equal to 2” to 5” H2O with a “TEE” connector and flexible tubing. Connect other end of valve to an electronic bubble meter or standard bubble tube with flexible tubing (See Fig. 2.1) . NOTE:
A light load can be a 5-μm filter and/or an adjustable valve.
Source: Wikisource

National Institute for Occupational Safety and Health NIOSH Manual of Analytical Methods… (1994)

Pass the filter over an anti-static radiation source. Repeat this step if filter does not release easily from the forceps or if filter attracts balance pan. Static electricity can cause erroneous weight readings. 3.
Assemble the filters in the filter cassettes and close firmly so that leakage around the filter will not occur. Place a plug in each opening of the filter cassette. 4.
Remove the cyclone’s grit cap before use and inspect the cyclone interior. If the inside is visibly scored, discard this cyclone since the dust separation characteristics of the cyclone may be altered.
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