National Institute for Occupational Safety and Health

Summary

National Institute for Occupational Safety and Health NIOSH Manual of Analytical Methods… (1994)

Agitate samples (on the shaker) for at least 12 h. Filter samples through a 0.8-μm cellulose ester membrane filter, saving the filtrate and resin. Place the collected resin and filter in a clean 50-mL beaker. Adjust filtrate pH to 8.0 ± 0.1 with 5 M NaOH, add more resin, then repeat steps 5 and 6, combining the filters and resins from the two extractions. Ash filters and resins in a low temperature oxygen plasma asher for 6 h or until ashing is NIOSH Manual of Analytical Methods (NMAM) , Fourth Edition, 8/15/94 METALS in urine: METHOD 8310, Issue 2, dated 15 August 1994 - Page 3 of 5
10. 11.
Source: Wikisource

National Institute for Occupational Safety and Health NIOSH Manual of Analytical Methods… (1994)

This method measures urine concentrations of metals. It is particularly useful for workers exposed to several metals simultaneously. This is a simultaneous, multielemental analysis, but is not compound specific.
INTERFERENCES: Spectral interferences are the primary interferences encountered in ICP-AES analysis. These are minimized by judicious wavelength selection and interelement correction factors. Background corrections are also made [1,2] .
OTHER METHODS: This method uses a measurement technique similar to that of Method 7300 (Elements by ICP) for air samples.
Source: Wikisource

Get perspective with Kwize: daily news enlightened by great literature