National Institute for Occupational Safety and Health

Summary

National Institute for Occupational Safety and Health,  NIOSH Manual of Analytical Methods… (1994)

“ Agitate samples (on the shaker) for at least 12 h. Filter samples through a 0.8-μm cellulose ester membrane filter, saving the filtrate and resin. Place the collected resin and filter in a clean 50-mL beaker. Adjust filtrate pH to 8.0 ± 0.1 with 5 M NaOH, add more resin, then repeat steps 5 and 6, combining the filters and resins from the two extractions. Ash filters and resins in a low temperature oxygen plasma asher for 6 h or until ashing is NIOSH Manual of Analytical Methods (NMAM) , Fourth Edition, 8/15/94 METALS in urine: METHOD 8310, Issue 2, dated 15 August 1994 - Page 3 of 5
10. 11.
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Source: Wikisource

National Institute for Occupational Safety and Health,  NIOSH Manual of Analytical Methods… (1994)

“ This method measures urine concentrations of metals. It is particularly useful for workers exposed to several metals simultaneously. This is a simultaneous, multielemental analysis, but is not compound specific.
INTERFERENCES: Spectral interferences are the primary interferences encountered in ICP-AES analysis. These are minimized by judicious wavelength selection and interelement correction factors. Background corrections are also made [1,2] .
OTHER METHODS: This method uses a measurement technique similar to that of Method 7300 (Elements by ICP) for air samples.
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Source: Wikisource

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