National Institute for Occupational Safety and Health

Summary

National Institute for Occupational Safety and Health NIOSH Manual of Analytical Methods… (1994)

Determine desorption efficiency (DE) at least once for each batch of Chromosorb 102 used for sampling in the calibration range (step 8) . Prepare three tubes at each of five levels plus three media blanks. a. Remove and discard back sorbent section of a media blank sampler. b. Inject a known amount of calibration stock solution directly onto front sorbent section with a microliter syringe. c. Cap the tube. Allow to stand overnight. d. Desorb (steps 5 through 7) and analyze together with working standards (steps 11 and 12) . e. Prepare a graph of DE vs. μg Mevinphos recovered.
Source: Wikisource

National Institute for Occupational Safety and Health NIOSH Manual of Analytical Methods… (1994)

Mevinphos is a cholinesterase inhibitor and can be absorbed through the skin. Wear protective gloves and suitable protective clothing when handling the pure material [1] .
SAMPLING: 1. 2. 3. 4.
Calibrate each personal sampling pump with a representative sampler in line. Break the ends of the sampler immediately before sampling. Attach sampler to personal sampling pump with flexible tubing.
Source: Wikisource

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