1911 Encyclopædia Britannica, Volume 14… (1911)
“ The double chloride is fused with nitre, the melt extracted with water and the residue fused with lead, the excess of lead being finally removed by solution in nitric acid and aqua regia. It is a brittle metal of specific gravity 22.4 (Deville and Debray) , and is only fusible with great difficulty. It may be obtained in the spongy form by igniting iridium ammonium chloride, and this variety of the metal readily oxidizes when heated in air. ”
