Sorbent

Definition and stakes

National Institute for Occupational Safety and Health,  NIOSH Manual of Analytical Methods… (1994)

“ Prepare calibration graph (peak height or area vs. μg diphenyl per sample) . Determine desorption efficiency (DE) at least once for each lot of sorbent used for sampling in the range of interest. Prepare three tubes at each of five levels plus three media blanks. a. Remove and discard back sorbent section of a media blank sampler. b. Inject 2 to 10 μL of DE stock solution (or of a serially diluted solution in hexane) directly onto front sorbent section with a microliter syringe. c. Cap the tube. Allow to stand overnight. ”
Source: Wikisource

National Institute for Occupational Safety and Health,  NIOSH Manual of Analytical Methods… (1994)

“ Weigh the dry sorbent and place it in a 250-mL round-bottom flask. 5. Weigh an amount of maleic anhydride equivalent to 20% of the weight of the sorbent and dissolve it in 50 mL acetone. 6. Add the maleic anhydride solution to the sorbent, swirl, and remove the solvent in a rotary evaporator. Dry in a vacuum oven at 30 °C for 15 min. Use the coated sorbent within 20 days of preparation. NOTE: Refrigeration in a sealed container may prolong shelf life [1,4] . ”
Source: Wikisource

Charles S. McCammon, Ph.D., CIH, NIOSH/Denver Field Office and Mary Lynn Woebkenberg, Ph.D., NIOSH/DPSE,  NIOSH Manual of Analytical Methods… (1994)

“ Use a bubble meter or equivalent flow measuring device.
(2) Break the ends of the solid sorbent tube immediately before sampling to provide an opening at least one-half of the internal diameter at each end. (3) Connect the solid sorbent tube to a calibrated personal sampling pump with flexible tubing with the smaller sorbent section (backup section) nearer to the pump. Do not pass the air being sampled through any hose or tubing before entering the solid sorbent tube. Position the solid sorbent tube vertically during sampling to avoid channeling and premature breakthrough.
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Source: Wikisource

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