Pierre Joseph Macquer,
Elements of the Theory and Practice of Chymistry…
“ The reason why the liquor that rises first contains a great deal more Volatile Salt than the other, in so much that it coagulates and becomes solid, is because the Volatile Salt rises in distillation much more easily than water.In whatever manner the Volatile Spirit or Salt be distilled from Sal Ammoniac, by means of a Fixed Alkali, we always find at the bottom of the retort, or cucurbit, when the operation is finished, a new Neutral Salt compounded of the Acid of the Sal Ammoniac, and of the Alkali used in the distillation. ”
